Patent No. EP4008699 (titled "Method For Producing Zirconia Sintered Compact") was filed by Kuraray Noritake Dental on Jul 31, 2020. The application was issued on Oct 16, 2024.
A method for producing a zirconia sintered body involves firing a zirconia molded or pre-sintered body through at least three temperature increase steps (H1, H2, H3). The first step (H1) starts at room temperature to 500°C and reaches 900 to 1250°C at a rate (HR1) of 50 to 500°C/min. The second step (H2) starts at 900 to 1250°C and reaches 1300 to 1550°C at a rate (HR2) of 11 to 300°C/min. The third step (H3) starts at 1300 to 1550°C and reaches 1400 to 1650°C at a rate (HR3) of 10 to 299°C/min. The process must satisfy HR1 > HR2 and HR2/HR3 > 1 to ensure optimal color tone, translucency, and strength in short-time firing.

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