3M Company et al. vs Westech Aerosol Company

Trial Certificate Checklist

3M Company¿¿¿s Notice of Cross-Appeal

DECISION Denying Petitioner's Request for Rehearing

Petitioners Request for Rehearing

FINAL WRITTEN DECISION 35 U.S.C. § 318(a) and 37 C.F.R. § 42.73

Hearing Transcript

Granting Petitioners Motion to Strike 37 C.F.R. sec 42.5

Patent Owner's Response to Petitioner's Motion to Strike

ORDER Trial Hearing Order 35 U.S.C. sec 316(a)(10) and 37 C.F.R. sec(s) 42.70

Petitioners Motion to Strike

Patent Owner Westech Aerosol Corporation's Request for Oral Argument

Petitioners Surreply to Patent Owner¿¿¿s Contingent Motion to Amend

3M Companys Request for Oral Argument

ORDER - Conduct of the Proceeding 37 C.F.R. ¿¿¿¿ 42.14 and 42.54

Petitioners Objections to Evidence Under 37 C.F.R. 42.64

Stipulated Motion to Seal

EXPUNGED

Patent Owner's Surreply

Diversified CPC International Inc., An Introduction to Aerosol Propellants

n-Hexane (Commercial Grade) Safety Data Sheet from Chevron Phillips, Rev. 2015-08-28

Mullin, Rick, Design of Experiments Makes a Comeback, C&EN, Vol. 91, Issue 13, p. 25-28, April 1, 2013

Hexane (S) - Safety Data Sheet from Phillips 66, Nov. 9, 2018

U.S. Patent No. 5,662,840 (Thomas et al.)

U.S. Patent No. 6,268,191 (Prud¿¿¿homme et al.)

Meyers, H.S., Vapor Pressure Chart for All Types of Low Boiling Hydrocarbons, Ind. & Eng. Chemistry, Vol. 47, No. 8, p. 1659-60 (1955)

HEXANES MSDS Number: H2370 ¿¿¿ Effective Date 12/08/96, safety data sheet

Deposition of Dr. Prud¿¿¿homme on March 20, 2019

Supplemental Declaration of Robert A. Wanat Ph.D.

Hexane, mixture of isomers- Safety Data Sheet from Sigma-Aldrich , 11/24/2017 Version 5.10

Hanlon et al., Handbook of Package Engineering, CRC Press (1998), excerpt (p. 383)

Preface (page xiv) from Russel et al., Colloidal Dispersions (Cambridge Monographs on Mechanic), Cambridge Univ Press (1989)

Redacted Declaration of Robert A. Wanat Ph.D.

40 CFR ¿¿ 799.2155 ¿¿¿ Commercial hexane

Wiley.com: introduction to Ferry, Viscoelastic Properties of Polymers, 3rd Edition, ISBN:978-0-471-04894-7 (1980), available at https://www.wiley.com/en-us/Viscoelastic+Properties+of+Polymers%2C+3rd+Edition-p-9780471048947

Redacted - Westech Batch Record for HSC-13 canister adhesive from August 2003

EXPUNGED

Westech's Updated Exhibit List

Patent Owner's Reply to Petitioner's Opposition to Patent Owner's Contingent Motion to Amend

ORDER Denying Patent Owner¿¿¿s and Petitioner¿¿¿s Motions to Seal (Papers 10, 12) 37 C.F.R. ¿¿¿¿ 42.14 and 42.54

Patent Owner's Notice of Deposition of Dr. Robert K. Prud'Homme

Motion to Seal Under 37 C.F.R. 42.14 and 42.54

Petitioner¿¿¿s Reply

Errata from 2018-10-11 Deposition of Dr. Robert K. Prud homme

Petitioners Opposition to Patent Owners Contingent Motion to Amend

Photo of Building

Rule 1168, Adhesive and Sealant Applications

Larson, R. G., The Structure and Rheology of Complex Fluids (1999)

Box, George, et al., Statistics for Experimenters: An Introduction to Design, Data Analysis, and Model Building (1978)

Russel, W. B., et al., Colloidal Dispersions Cambridge University Press, 466 (1989)

Ferry, J.D., Viscoelastic Properties of Polymers (1980)

Sperling, L. H., Introduction to Physical Polymer Science (1992)

Wendt, P., The Control of Rubber in World War II (1947)

U.S. Patent No. 2,595,797 (Leyonmark)

U.S. Patent No. 5,997,952 (Harris)

U.S. Patent No. 6,191,211 (Mussell)

U.S. Patent No. 3,238,173 (Bailey)

2019-02-15 Deposition Transcript of Dr. Robert Wanat, Ph.D., Filed Under Seal

EXPUNGED

Rubber Matters: Solving the World War II Rubber Problem, Wartime Crisis

Krieger, I. M., and Dougherty, T. J., A Mechanism for Non-Newtonian Flow in Suspensions of Rigid Spheres (1959)

Smith, J. M., and Van Ness, H. C., Introduction to Chemical Engineering Thermodynamics (1987)

Butera, R., et al., Microscopic and Macroscopic Evaluation of Fundamental Facets of the Entanglement Concept (1991)

Long, C., and Prud¿¿¿homme, R., Microencapsulation of Aqueous Compounds Using Hexamethylenediamine and Trimesoyl Chloride: Monodisperse Capsule Formation and Reaction Conditions on Membrane Properties (2014)

Aminabhavi, T. M., et al., Rubber ¿¿¿ Solvent Interactions (1991)

Morris, E. R., et al., Concentration and Shear Rate Dependence of Viscosity in Random Coil Polysaccharide Solutions (1981)

Fox, T. G., and Allen, V. R., Dependence of the Zero Shear Melt Viscosity and the Related Friction Coefficient and Critical Chain Length on Measurable Characteristics of Chain Polymers (1964)

Grassley, W. W., et al., Packing Length Influence in Linear Polymer Melts on the Entanglement, Critical, and Reptation Molecular Weights (1999)

Bares, J. Glass Transition of Polymer Microphase (1974)

Pico, E. R., and Williams, M.C., Solvation and Phase Separation in ABA Block Copolymers (1978)

Matsuo, M. et. Al., Fine Structures and Fracture Processes in Plastic-Rubber Two-Phase Polymer Systems (1970)

Expert Declaration of Robert K. Prud homme, Ph.D. in Support of Petitioner¿¿¿s Reply and Opposition to Contingent Motion to Amend

3M Companys Updated Exhibit List

Fetters, L. J., et al., Connection between Polymer Molecular Weight, Density, Chain Dimensions, and Melt Viscoelastic Properties (1994

Notice of Joint Stipulation to Modify Due Dates 2 through 4

Order Conduct of the Proceeding

3M Companys Updated Mandatory Notices

Decision - Granting Petitioner's Motion for Pro Hac Vice Admission of Melissa R. Gibson - 37 CFR 42.10(c)

EXPUNGED

Decision - Granting Petitioner's Motion for Pro Hac Vice Admission of Michael P. Kahn - 37 CFR 42.10(c)

SECOND AMENDED SCHEDULING ORDER 37 C.F.R. sec. 42.5(a)

Declaration of Melissa R. Gibson in Support of Motion to Appear Pro Hac Vice

Petitioners Motion for Pro Hac Vice Admission of Michael P. Kahn

Declaration of Michael P. Kahn in Support of Motion to Appear Pro Hac Vice

Petitioners Motion for Pro Hac Vice Admission of Melissa R. Gibson

3M Companys Updated Exhibit List

Petitioners Notice of Deposition of Robert A. Wanat, Ph.D.

Petitioners Objections to Evidence Under 37 C.F.R. 42.64

Exhibit 2004

Exhibit 2006

Exhibit 2008

Exhibit 2009

U.S. EPA Project Summary, ¿¿¿Solvent-Based to Waterbased Adhesive-Coated Substrate Retrofit¿¿¿ EPA/600/SR-95/011 (June 1996)

Petrie, Edward, ¿¿¿Water-Based Vs. Solvent-Based Adhesives,¿¿¿ Article, (February 2003)

A Concise Dictionary of Chemistry, Oxford University Press, New Edition (1990)

Carraher, Charles E., Jr., Polymer Chemistry, Sixth Edition (Revised and Expanded), Marcel Dekker, Inc. (2003)

Kulicke, Werner-Michael, Viscosimetry of Polymers and Polyelectrolytes, Springer-Verlag Berlin Heidelberg New York (2004)

Exhibit 2002

Exhibit 2003

Exhibit 2005

Exhibit 2007

Exhibit 2010

ESCOREZ¿¿¿ 5000 Series, Technical Data Sheet, Exxon Mobile (April 2018)

Bullard, Jeffrey W. et. al., ¿¿¿A Comparison of Viscosity-Concentration Relationships for Emulsions¿¿¿

ASI Adhesives & Sealants Indus. Magazine, Polychloroprene Contact Adhesives: Water-based adhesive systems make inroads into traditional solventborne technology, (March 2003)

Byutner, Oleksiy, et. al. Temperature and Molecular Weight Dependence of the Zero Shear-Rate Viscosity of an Entangled Polymer Melt from Simulation Theory, J. Polym. Sci. Part B: Polym. Phys.: Vol 39 (2001)

Smith-Romagnoli, V.L., Control of Spray Drop Size by Rheology, PhD Dissertation, Dept. Chem. Engineering, Princeton University (2001)

Lee, Shau-Tang, Polymeric Foams: Innovations in Processes, Technologies, and Products CRC Press Taylor & Francis Group Publishers (2017)

Guomin, Jiang, Aerosol Propellant Handbook, Cosmos Books Ltd., (1998)

Kraton Polymer Brochure (March 2001)

Declaration of Robert A. Wanat Ph.D.

EXPUNGED

Mosen, N.M., Effects of curing time and filler concentration on curing and postcuring of urethane dimethacrylate composites: A microcalorimetric study John Wiley & Sons, Inc. (1998)

Mayzo Antioxidant Technical Data Sheet

Report of Lab/Cor Materials LLC date November 29, 2018

Declaration of Robert A. Wanat Ph.D. in Support of Contingent Motion to Amend

Solubility Parameters: Theory and Application - The Book and Paper Group, Vo.3 (1984) (available at https://cool.conservation-us.org/coolaic/sg/bpg/annual/v03/bp03-04.html)

Vega, Daniel, A. et. al. Phase Behavior and Viscoelastic Properties of Entangled Block Copolymer Gels, Journal of Polymer Science: Part B: Polymer Physics, Vol. 39, 2183¿¿¿2197 (2001)

Westech Batch Record for HSC-13 canister adhesive from August 2003

Lambourne, R., et. al., Paint and Surface Coatings, Theory and Practice, Woodhead Publishing Ltd. (1999)

Deposition of Dr. Robert Prud¿¿¿Homme

Johnsen, Monfort A., The Aerosol Handbook (2nd Ed.) Wayne Dorland Company (1982)

Encylcopedia.com entry for SBS, https://www.encyclopedia.com/science/academic-and-educational-journals/polystyrene-butadiene-styrene (last visited November 8, 2018)

Summary of Minutes from The South Coast Air Quality Management District, June 7, 2002 (available at http://www3.aqmd.gov/hb/2002/July/0206min.html) (last visited November 8, 2018)

Summary of Minutes from The South Coast Air Quality Management District, May 3, 2002 (available at http://www3.aqmd.gov/hb/2002/June/0205min.html) (last visited November 8, 2018)

Summary of Minutes from The South Coast Air Quality Management District, September 21, 2001 (available at http://www3.aqmd.gov/hb/2001/October/0109min.html) (last visited November 8, 2018)

Administrative Records of the South Coast Air Quality Management District, Rule 1168 ADOPTED/AMENDMENTS FROM 4/7/1989-10/3/2003

ASI Adhesives & Sealants Indus. Magazine Westech Wins Environmental Leadership Award (September 2003)

WO1999060042A1 (Nissen)

Naugard Antioxidant Technical Data Sheet

U.S. 8,137,699 (Johnson)

Introduction to Factorial Experimental Designs - Penn State, (available at https://methodology.psu.edu/ra/most/factorial)

Westech Product Brochure

Patent Owner's Motion to Seal

Patent Owner's Response Under 37 C.F.R. ¿¿ 42.120

Patent Owner's Contingent Motion to Amend Under 37 C.F.R. ¿¿42.121

Notice of Joint Stipulation to Modify Due Dates 1-5

Amended Scheduling Order

Decision Institution of Inter Partes Review

Scheduling Order

Richard J. Lewis, HAWLEY'S CONDENSED CHEMICAL DICTIONARY 461 (Van Nostrad Reinhold 1993)

LINUS PAULING, GENERAL CHEMISTRY 476, (1988)

John Daintith, A DICTIONARY OF CHEMISTRY

Expert Declaration of Dr. Kenneth Brown

US Patent No. 5,711,484 (Blette)

US Patent No. 5,159,894 (Saidman)

US Patent No. 4,301,119 (Cobbs)

Patent Owner's Preliminary Response

PATENT OWNER'S MANDATORY NOTICE UNDER 37 C.F. R. ¿¿ 42.8

Notice of Accord Filing Date

U.S. Patent No. 7,705,056 (the 056 Patent)

Affidavit of Translation of Japanese Patent Application Publication No. H11-349917

Petition for Inter Partes Review

U.S. Patent Application No. 10/979,575 (CIP Application)

U.S. Publication No. 2002/0161056 (Carnahan Publication)

U.S. Patent No. 5,480,925 (Masuzaki)

Petrie, Handbook of Adhesives and Sealants, McGraw-Hill, 2000

Huggins, Molecular Interactions in Pure Liquids and Solutions, Symposium on Energy Concepts, 41(536):509, 1969

Weiss, Paint and Coatings: A Mature Industry in Transition, Prog. Polym. Sci., 22:203, 1997

Ferry, Viscoelastic Properties of Polymers 3d Ed., John Wiley & Sons, Inc., 1980

Order dismissing Case No. 3:17-cv-05067-RBL without prejudice

Acetone CAS No: 67-64-1

Certified English Translation of Japanese Patent Application Publication No. H11-349917 (Takashima)

Petitioners Power of Attorney

Prosecution History of Application No. 10/979,575 that led to the 056 Patent

Expert Declaration of Robert K. Prud homme, Ph.D.

U.S. Patent No. 5,931,354 (Braud)

Japanese Patent Application Publication No. H11-349917

U.S. Provisional Application No. 60/287,671 (Provisional Application)

U.S. Patent Application No. 10/132,620 (Parent Application)

Prosecution History of Parent Application

Comparison of Parent Application and CIP Application

Comparison of Provisional Application and the Parent Application

Comparison of Carnahan Publication and the ¿¿¿056 Patent

U.S. Patent No. 3,400,095 (Kremer)

U.S. Patent No. 3,578,622 (Brown)

U.S. Patent No. 4,228,933 (Elson)

U.S. Patent No. 4,401,271 (Hansen)

U.S. Patent No. 5,066,522 (Cole)

U.S. Patent No. 5,118,750 (Silver)

U.S. Patent No. 5,444,112 (Carnahan 112)

European Patent Application 0814139 (Purvis)

Brandrup et al., Polymer Handbook 2d ed., John Wiley & Sons, 1975 (Brandrup)

Burke, Solubility Parameters: Theory and Applications, The Book and Paper Group Annual, 3:13 (1984)

Takahashi et al., Zero-Shear Viscosity of Linear Polymer Solutions over a Wide Range of Concentration, Macromolecules, 18:1002 (1985)

The Science and technology of Aerosol Packaging, Edited by J. Sciarra & L. Stoller, John Wiley & Sons, Inc., 1974

Sanders, Principles of Aerosol Technology, Van Nostrand Reinhold Company, 1970

Summons to 3M in Westech Aerosol Corporation, etc., Pltf. Vs. 3M Company, etc. and GTA-NHT, Inc., etc., Dfts

Felder, Elementary Principles of Chemical Processes, 2nd Edition, 1986

N-Hexane - Material Safety Data Sheet

Cyclohexane ¿¿¿ Material Safety Data Sheet

Dombrowski, The Aerodynamic Instability and Disintegration of Viscous Liquid Sheets