Termination Decision Document | Oct 1, 2020 | PAPER | BOARD |
Petitioner's Notice of Deposition of Christopher J. Welch, PH.D Under 37 C.F.R. Section 42.53 | Sep 23, 2020 | PAPER | PETITIONER |
Joint Motion to Terminate Pursuant to 35 U.S.C. Section 317 and 37 C.F.R. Section 42.74 | Sep 18, 2020 | PAPER | PETITIONER |
Joint Request to File Covenant Not to Sue as Business Confidential Information Pursuant to 35 U.S.C. Section 317(b) and 37 C.F.R. Section 42.74(c) | Sep 18, 2020 | PAPER | PETITIONER |
Covenant Not to Sue [Confidential] | Sep 18, 2020 | EXHIBIT | PETITIONER |
Joint Stipulation and Order of Voluntary Dismissal with Prejudice | Sep 18, 2020 | EXHIBIT | PETITIONER |
Petitioner's Objections to Evidence Submitted with Patent Owner's Response | Jul 21, 2020 | PAPER | PETITIONER |
Patent Owner's Response | Jul 14, 2020 | PAPER | PATENT OWNER |
July 1, 2020 Deposition Transcript of Robert L. Fitzgerald,
Ph.D. | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Declaration of Dr. Christopher J. Welch, Ph.D. in Support of Patent
Owner¿¿¿s Response to Inter Partes Review of U.S. Patent No.
7,972,868 | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
June 30, 2020 Deposition Transcript of Robert D. Voyksner,
Ph.D. | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Karlson, P., et al., IUPAC-IUB Joint Commission on Biochemical Nomenclature (JCBN): nomenclature of vitamin D--recommendations 1981, Eur. J. Biochem. (1982) | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
March J., Advanced Organic Chemistry, 3rd Ed., John Wiley & Sons. (1985). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Knapp, D.R., Handbook of Analytical Derivatization Reactions, John Wiley & Sons. (1979). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Norman, A.W., Sunlight, season, skin pigmentation, vitamin D, and 25-hydroxyvitamin D: integral components of the vitamin D endocrine system, Am J Clin Nutr., 67:1108¿¿¿10 (1998). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
SciFinder literature search results for 4'-carboxyphenyl-TAD. | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Memorandum Order addressing claim construction in Civil Action
No. 1:18-cv-01436 (MN) on January 14, 2020. | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
van den Ouweland, JMW. Analysis of vitamin D metabolites by liquid chromatography-tandem mass spectrometry. TrAC Trends in Analytical Chemistry 84:117-130 (2016). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Aronov et al., Metabolic profiling of major vitamin D metabolites using Diels-Alder derivatization and ultra-performance liquid chromatography-tandem mass spectrometry, Anal. Bioanal. Chem. 391(5):1917-1930 (2008). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
NIH PubChem entry for 1,4-Phthalazinedione structure, available at https://pubchem.ncbi.nlm.nih.gov/compound/1_4-Phthalazinedione (last accessed July 10, 2020). | Jul 14, 2020 | EXHIBIT | PATENT OWNER |
Patent Owner's Notice of Deposition of Dr. Robert L. Fitzgerald | Jun 16, 2020 | PAPER | PATENT OWNER |
Patent Owner's Notice of Deposition of Dr. Robert Voyksner | Jun 16, 2020 | PAPER | PATENT OWNER |
Joint Stipulation to Adjust the Scheduling Order | May 14, 2020 | PAPER | PATENT OWNER |
Trial Instituted Document | Mar 20, 2020 | PAPER | BOARD |
Scheduling Order | Mar 20, 2020 | PAPER | BOARD |
Petitioner's Updated Mandatory Notice Pursuant to 37 C.F.R. Section 42.8 | Feb 14, 2020 | PAPER | PETITIONER |
Patent Owner's Preliminary Response | Dec 24, 2019 | PAPER | PATENT OWNER |
Statutory Disclaimer under 35 U.S.C. ¿¿ 253(a) | Dec 24, 2019 | EXHIBIT | PATENT OWNER |
Vreeken, R.J. et al., On-line post-column Diels-Alder derivatization for the determination of vitamin D3 and its metabolites by liquid chromatography/thermospray mass spectrometry, Biol. Mass. Spec., 22, 621-632 (1993) | Dec 24, 2019 | EXHIBIT | PATENT OWNER |
Joint Claim Construction Chart - Exhibit A filed in Civil Action No. 1:18-cv-01436-MN | Dec 24, 2019 | EXHIBIT | PATENT OWNER |
Loudon, M.G., Organic Chemistry, 3rd ed. (1995) | Dec 24, 2019 | EXHIBIT | PATENT OWNER |
Granting Patent Owner¿¿¿s Motions for
Admission Pro Hac Vice of Thomas H. Wintner
37 C.F.R. sec. 42.10 | Dec 20, 2019 | PAPER | BOARD |
Patent Owner's Unopposed Motion for Pro Hac Vice Admission of Thomas H. Wintner | Oct 22, 2019 | PAPER | PATENT OWNER |
Declaration of Thomas H. Wintner in Support of Motion for Pro Hac Vice Admission | Oct 22, 2019 | EXHIBIT | PATENT OWNER |
NOTICE OF ACCEPTING CORRECTED PETITION | Sep 30, 2019 | PAPER | BOARD |
Patent Owner's Power of Attorney | Sep 27, 2019 | PAPER | PATENT OWNER |
Patent Owner's Mandatory Notices | Sep 27, 2019 | PAPER | PATENT OWNER |
[Replacement] Higashi et al., Characterization of Urinary Metabolites of Vitamin D3 in Man under Physiological Conditions Using Liquid Chromatography-Tandem Mass Spectrometry, J. Pharm. Biomed. Anal. 29:947-55 (2002) | Sep 26, 2019 | EXHIBIT | PETITIONER |
Corrected Petition for Inter Partes Review | Sep 26, 2019 | PAPER | PETITIONER |
Notice of Accord Filing Date | Sep 25, 2019 | PAPER | BOARD |
Petition for Inter Partes Review | Sep 17, 2019 | PAPER | PETITIONER |
U.S. Patent No. 7,972,868 to Holmquist et al. | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Robert L. Fitzgerald, Ph.D., DABCC | Sep 17, 2019 | EXHIBIT | PETITIONER |
File History for U.S. Patent No. 7,972,868 to Holmquist et al. | Sep 17, 2019 | EXHIBIT | PETITIONER |
Higashi et al., Characterization of Urinary Metabolites of Vitamin D3 in Man under Physiological Conditions Using Liquid Chromatography-Tandem Mass Spectrometry, J. Pharm. Biomed. Anal. 29:947-55 (2002) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Kobayashi et al., Production of a Group-Specific Antibody to 1 a,25-Dihydroxyvitamin D and Its Derivatives Having the 1 a,3 b-Dihydroxylated A-Ring Structure, Steroids 59:404-11 (1994) | Sep 17, 2019 | EXHIBIT | PETITIONER |
U.S. Patent No. 6,787,660 to Armbruster et al. | Sep 17, 2019 | EXHIBIT | PETITIONER |
Kobayashi et al., Tandem Immunoaffinity Chromatography, J. Steroid Biochem. Molec. Biol. 54:217-26 (1995) (Kobayashi 1995) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Dr. Robert Voyksner | Sep 17, 2019 | EXHIBIT | PETITIONER |
Honour, High-Performance Liquid Chromatography for Hormone Assay Chapter 2 in Methods in Molecular Biology: Hormone Assays in Biological Fluids, 25-51 (M.J. Wheeler & J.S.M. Hutchinson, eds., 2006) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Fitzgerald and Herold, Serum Total Testosterone: Immunoassay Compared with Negative Chemical Ionization Gas Chromatography Mass Spectrometry, Clin. Chem. 42(5):749-55 (1996) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Kissmeyer and Sonne, Sensitive Analysis of 1,25-Dihydroxyvitamin D3 in Biological Fluids by Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatography A 935:93-103 (2001) | Sep 17, 2019 | EXHIBIT | PETITIONER |
A. Michael Parfitt, Osteomalacia and Related Disorders, in Metabolic Bone Disease and Clinically Related Disorders,329-96 (Aviolo, Krane, eds., 3rd ed. 1997) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Armas et al., Vitamin D2 is Much Less Effective than Vitamin D3 in Humans, J. Clin. Enodcrinol. & Metab., 89:5387-91(2004) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Kissmeyer et al., Determination of the Vitamin D Analog EB 1089 (Seocalcitol) in Human and Pig Serum Using Liquid Chromatography-Tandem Mass Spectrometry, J. Chromatog. B, 740:117-28 (2000) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Fitzgerald et al., Broad Spectrum Drug Identification Directly from Urine, Using Liquid Chromatography-Tandem Mass Spectrometry, Clin. Chem., 45:1224-34 (1999) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Tsugawa et al., Determination of 25-Hydroxyvitamin D in Human Plasma Using High-Performance Liquid Chromatography-Tandem Mass Spectrometry, Anal. Chem. 77:3001-07 (2005) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Yeung et al., Characterization of Vitamin D3 Metabolites Using Continuous-Flow Fast Atom Bombardment Tandem Mass Spectrometry and High-Performance Liquid Chromatography, J. Chromatography 645:115-23 (1993) | Sep 17, 2019 | EXHIBIT | PETITIONER |
U.S. Patent No. 6,399,796 to Schwartz | Sep 17, 2019 | EXHIBIT | PETITIONER |
Reserved | Sep 17, 2019 | EXHIBIT | PETITIONER |
Higashi et al., Electron-Capturing Derivatization of Neutral Steroids for Increasing Sensitivity in Liquid Chromatography/Negative Atmospheric Pressure Chemical Ionization-Mass Spectrometry, Anal. Sci. 18:1301-07 (2002) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Higashi et al., Application of 4-(4-Nitrophenyl)-1,2,4-triazoline-3,5-dione to Analysis of 25-Hydroxyvitamin D3 in Human Plasma by Liquid Chromatography/Electron Capture Atmospheric Pressure Chemical Ionization-Mass Spectrometry, Anal. Sci. 19:941-43 | Sep 17, 2019 | EXHIBIT | PETITIONER |
Vogeser, Liquid Chromatography-Tandem Mass Spectrometry Application in the Clinical Laboratory, Clin. Chem. Lab. Med. 41(2):117-26 (2003) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Patrick Gordis (for Tsugawa) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Patrick Gordis (for Yeung) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Patrick Gordis (for Higashi) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Declaration of Patrick Gordis (for Kobayashi) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Legrand et al., Measurement of plasma testosterone by gas chromatography-negative-ion mass spectrometry using pentafluoropropionic derivatives, J. Chromatog. 663:187-92, 189 (1995) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Rainbow et al., The Analysis of Vitamin D Analogues by Atmospheric Pressure Ionization Coupled to TripleQuadrupole Mass Spectrometry, Poster No. M-045, Proceedings of the 51st ASMS Conference on Mass Spectrometry and Allied Topics, Montreal, Canada | Sep 17, 2019 | EXHIBIT | PETITIONER |
Trivedi et al., Effect of Four Monthly Oral Vitamin D3 (Cholecalciferol) Supplementation of Fractures and Mortalityin Men and Women Living in the Community: Randomised Double Blind Controlled Trial, BMJ 326:469-74 (2003) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Food and Nutrition Board, Institute of Medicine, Dietary Reference Intakes For Calcium, Magnesium, Phosphorus,Vitamin D and Fluoride, 250-287 (National Academy Press,
1997) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Herbert and Johnstone, Mass Spectrometry Basics 225-35, 245-52, 261-68, and 413-15 (CRC Press LLC, 2002) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Hollis and Napoli, Improved Radioimmunoassay for Vitamin D and Its Use in Assessing Vitamin D Status, Clin. Chem. 31(11):1815-19 (1985) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Fitzgerald et al., Comparison of an Ion ¿¿¿Trap and a Quadrupole Mass Spectrometer using Diazepam as a Model Compound, J. Analytical Toxicology, 21:445-50 (1997) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Voyksner and Lee, Improvements in LC/Electrospray Ion Trap Mass Spectrometry Performance Using an Off-Axis Nebulizer, Anal. Chem. 71:1441-47 (1999) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Glenville Jones and Hugh L.J. Makin, ¿¿¿Vitamin Ds: Metabolites and Analogues,¿¿¿ Chapter 2 in Modern Chromatographic Analysis of Vitamins, 87-153 (Leenheer, Lambert & Van Bocxlaer, eds., 3rd ed. 2000) | Sep 17, 2019 | EXHIBIT | PETITIONER |
Creaser et al., Immunoaffinity Chromatography Combined On-Line with High Performance Liquid Chromatography-Mass Spectrometry for the Determination of Corticosteroids, J. Chromatography A 794:37-43 (1998) | Sep 17, 2019 | EXHIBIT | PETITIONER |
National Library of Medicine, PubChem Computed Properties for Calcitriol | Sep 17, 2019 | EXHIBIT | PETITIONER |
Power of Attorney | Sep 17, 2019 | PAPER | PETITIONER |