Solvay USA Inc. et al. vs World Sources Enterprises, LLC

Other: Fed Circuit mandate

Other: other court decision

Notice of Appeal

Updated Mandatory Notices

JUDGMENT Final Written Decision Determining All Claims Unpatentable DECISION Denying Patent Owner’s Request for Rehearing ORDER Dismissing Petitioner’s Motion to Exclude Evidence

MOTION FOR RECONSIDERATION AND REHEARING OF PATENT OWNER¿¿¿S MOTION FOR ADDITIONAL DISCOVERY AND OBJECTION TO EXHIBIT 1006

Order - Denying Patent Owner's Combined Motion for Additional Discovery and Late-Filed Objection to Exhibit 1006 - 37 CFR 42.5(c)(3), 42.224(a)

Hearing Transcript

Petitioner's Opposition to Patent Owner's Motion for Additional Discovery

Exhibit 2091 LinkedIn Page of Kayla Garcia

Motion for additional discovery and objection to Exhibit 1006

Order Conduct of the Proceeding

Email

Petitioner's Oral Argument Demonstratives

Joint Objections to Demonstratives

Patent Owner demonstrative exhibits

Petitioner¿¿¿s Reply to Patent Owner¿¿¿s Response to Petitioner¿¿¿s Motion to Exclude

Trial Hearing 37 C.F.R. ¿¿ 42.70

PATENT OWNERS¿¿¿ RESPONSE TO MOTION TO EXCLUDE

Patent Owner's Request for Oral Hearing

Petitioner's Motion to Exclude

Petitioner's Request for Oral Argument

Exhibit 2006 Part I

Exhibit 2006 Part II

Order - Conduct of the Proceeding

Motion to substitute sur reply

Sur-reply with 5600 word limit

Motion to substitute Image for Document 41

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Deposition Transcript of Thomas Theyson, January 17, 2020

Deposition Transcript of Raymond Perkins, January 13, 2020

Petitioner Reply to Patent Owner Response

Updated Mandatory Notices

Power of Attorney by Patent Owner

Motion for Pro Hac Vice admittance of David Wilkerson

Updated declaration of David Wilkerson

Order Conditionally Granting Patent Owner's Motion for Admission Pro Hac Vice of David M. Wilkerson

Patent Owners¿¿¿ Motion for Pro Hac Vice Admission of David M. Wilkerson Under 37 C.F.R. ¿¿ 42.10

Declaration of David M. Wilkerson REGARDING U.S. PATENT NO. 10,221,108

Petitioner's Notice of Deposition

Petitioner's Notice of Deposition of Raymond Perkins

Petitioner's Notice of Deposition of Randall Rayborn

ORDER Conduct of the Proceeding 37 C.F.R. ¿¿ 42.5

Petitioner's Objections to Evidence

Motion to excuse late action

Exhibit 2088 Schroeder Declaration

Patentee Response

Exhibit 2014 Patent History of NBPT and its solvent delivery systems.

Exhibit 2016 Novelty Obviousness Continuum Drawing

Exhibit 2020 Evolution Timeline of Delivery Systems for NBPT-1

Exhibit 2023 Declaration of Randall Linwood Rayborn regarding chill point testing of a NMP containing solvent delivery system product and a DMSO-containing product

Exhibit 2024 GB Patent No. 898302A

Exhibit 2028 Whitehurst ¿¿¿189 US Patent No. 8,048,189

Exhibit 2031 Dimethyl sulfoxide Safety Data Sheet

Exhibit 2032 N-methyl Pyrrolidone Safety Data Sheet

Exhibit 2015 Expert Report of Thomas Theyson, Ph.D.

Exhibit 2017 Iannotta¿¿¿806 permutations of Solvents.

Exhibit 2018 CN¿¿¿400 drawings showing process of CN¿¿¿400

Exhibit 2019 Declaration of William Ulrich regarding available NBPT products on the market during the time of the filing of McKnight¿¿¿108

Exhibit 2021 Evolution of Solvent Systems

Exhibit 2022 Declaration of Ray Perkins regarding estimated sales of NBPT

Exhibit 2025 GB Patent No. 830800A

Exhibit 2026 Cigler ¿¿¿425 U.S. Patent No. 8,617,425

Exhibit 2027 Whitehurst ¿¿¿058 U.S. Patent No. 8,163,058

Exhibit 2029 Sutton ¿¿¿803 U.S. Patent No. 9,102,803

Exhibit 2030 Weston ¿¿¿265 U.S. Patent No.5, 352,265

Exhibit 2033 N-(n-butyl) thiophosphoric triamide Safety Data Sheet

Exhibit 2034 Acetone Safety Data Sheet

Exhibit 2035 Methanol Safety Data Sheet

Exhibit 2036 Ethanol Safety Data Sheet

Exhibit 2037 Isopropanol Safety Data Sheet

Exhibit 2038 Diisobutyl Ketone Safety Data Sheet

Exhibit 2039 Benzene Safety Data Sheet

Exhibit 2041 Chlorobenzene Safety Data Sheet

Exhibit 2042 Xylene Safety Data Sheet

Exhibit 2044 Tetrahydrofuran Safety Data Sheet

Exhibit 2045 Diethyl ether Safety Data Sheet

Exhibit 2059 California Pamphlet N-Methylpyrrolidone Health Hazard Advisory from June 2014 issued by California Department of Public Health.

Exhibit 2060 McCallen, Matthew William Thesis, Wheat, Rice And Corn Response To The Urease Inhibitor N-(n-butyl Thiophosphoric Triamide) in a Dimethyl Sulfoxide/Propylene Glycol Solution ¿¿¿ December 2014 West Texas A & M University.

Exhibit 2061 Agrotain Product label showing instability at low temperatures.

Exhibit 2065 Gavilon Arborite Brochure

Exhibit 2066 N-Edge-Label Brochure

Exhibit 2068 CHS SunBasin Growers praise N Edge Brochure

Exhibit 2072 PinnitMax-Safety Data Sheet-1

InnovarAg Web Site Praise

Exhibit 2074 Importation Data on NBPT from Ports of Unloading in the United States since 2009

Exhibit 2077 E-mail from Alan Nix to David McKnight on October 30, 2019 regarding 100XP fluidized bed and price associated with testing.

Exhibit 2078 100XP Brochure.

Exhibit 2079 Search results from USPTO dated November 4, 2019 showing Petitioner has 10 patent applications with DMSO and NBPT.

Exhibit 2080 E-mail string ending October 30, 2019 to and from Ray Perkins showing that Rhodiasolv ¿¿¿ LI-TEC is discontinued

Exhibit 2040 Toluene Safety Data Sheet

Exhibit 2043 Dimethylformamide Safety Data Sheet

Exhibit 2046 Dioxane Safety Data Sheet

Exhibit 2047 Carbon tetrachloride Safety Data Sheet

Exhibit 2048 Methylene chloride Safety Data Sheet

Exhibit 2049 Octane Safety Data Sheet

Exhibit 2050 Heptane Safety Data Sheet

Exhibit 2051 Hexane Safety Data Sheet

Exhibit 2052 Phosphorous oxychloride Safety Data Sheet

Exhibit 2053 Thiophosphoryl chloride Safety Data Sheet

Exhibit 2054 Dimethyl Sulfoxide (DMSO): A Review, Brayton Cory F., Cornell Vet, 1986, 76: p. 61

Exhibit 2055 DBE-5 Dibasic Ester SDS

Exhibit 2056 Sitarek et al. Tissue distribution and excretion of N-methyl-2-pyrrolidone in male and female rats. Int J Occup Med Environ Health. 2006;19(2):142-8.

Exhibit 2057 Sitarek et al. Assessment of reproductive toxicity and gonadotoxic potential of N-methyl-2-pyrrolidone in male rats. Int J Occup Med Environ Health. 2008;21(1):73-80.

Exhibit 2058 ZareNezhad, Bahman, Effects of Process Variable on the Caking Tendency of Prilled Urea in the Warehouse of Urea Production Plants, Journal of the University of Chemical Technology and Metallurgy, 42, 1, 2007, p. 45-50.

Exhibit 2062 Arborite-AG-Brochure

Exhibit 2063 Cipher Label and SDS information

Exhibit 2064 Cipher Trademark Registration Data

Exhibit 2067 N-edge Trademark Registration Data

Exhibit 2069 N-Yield Press release

Exhibit 2070 PinnitMax Brochure

Exhibit 2071 PinnitMax_Specimen_Label

Exhibit 2075 E-mail from Scott Peeden sent to David McKnight on October 31, 2019 regarding CN¿¿¿400 testing.

Exhibit 2076 Letter from Alan Nix to David McKnight on October 2, 2019 regarding McKnight¿¿¿108 testing using non 100XP instrument.

Exhibit 2081 Arborite Trademark Registration Data

Exhibit 2082 Sun 27 Product Label and Press release

Exhibit 2083 Gaylord Chemical Company, LLC brochure, dimethyl solubility data, 2014.

Exhibit 2085 Comparison of the solvents in Iannotta¿¿¿806 and Ortiz-Suarez ¿¿¿140.

Exhibit 2086 SDS of Rhodiasolv LI-TEC v2 (appears to have changed relative to Rhodiasolv LI-TEC).

Exhibit 2084 Albemarle Fine Chemistry Services expands in Tyrone, Pennsylvania, 2012.

Exhibit 2087 Patentee¿¿¿s preliminary response filed May 17, 2019.

Petitioner's Updated Power of Attorney

Petitioner's Updated Mandatory Notices

Granting Institution of Post-Grant Review 35 U.S.C. sec 324(a)

SCHEDULING ORDER

Petition for Post-Grant Review, dated April 26, 2019 (as served on Patent Owner)

Clemens Anklin, NMR ¿¿¿ past, present and future Bruker February 2019

Prosecution history of U.S. Application No. 15/636,211

American Heritage Definition of ¿¿¿Suspension¿¿¿, Second College Edition, Houghton Mifflin Company, Boston, 1982, p. 1225.

Preliminary Response to Petition for Post Grant Review

University of Wisconsin NMR document ¿¿¿ Sensitivity in NMR October 26, 2009

Prosecution history of U.S. Application No. 15/793,326

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Prosecution history of U.S. Patent No. 9,266,789 (Ortiz-Saurez)

Prosecution history of U.S. Patent No. 9,266,789 (Ortiz-Saurez)

U.S. Patent No. 9,266,789 (Ortiz-Saurez)

U.S. Provisional Patent Application 61/708,105 (McKnight)

U.S. Provisional Patent Application 61/739,869 (Ortiz-Saurez)

U.S. Provisional Patent Application 61/834,544 (Ortiz-Saurez)

Differences in physical properties between deuterated DMSO and non-deuterated DMSO.

Power of attorney document

Mandatory Notices document

Notice of Accord Filing Date

Declaration of Gordon W. Gribble

U.S. Patent No. 10,221,108

US Patent No. 10,221,108 File History

U.S. Provisional Application No. 61/708,105

U.S. Patent Publication No. 2013/0145806 to Iannotta et al.

U.S. Provisional Application No. 61/630,456

U.S. Patent No. 5,698,003 to Omilinsky et al.

Zaman et al., ¿¿¿Effect of urease and nitrification inhibitors on N transformation ¿¿¿¿¿¿

Ullmann¿¿¿s Encyclopedia of Industrial Chemistry ¿¿¿ Sulfones and Sulfoxides entry (2012)

Engel, ¿¿¿Volatilization losses from surface-applied urea during cold weather months¿¿¿ (2011)

Martin et al., ¿¿¿The Solvent Dimethyl Sulfoxide¿¿¿

Organic Chemistry, C. M. Loudon, 2002, 4th ed., Oxford (excerpted pages)

Organic Chemistry, R. J. Fessenden, J. S. Fessenden, 1986, 3rd ed., Brooks/Cole (excerpted pages)

Organic Chemistry, M. A. Fox, J. K. Whitesell, 1997, 2nd ed., Jones and Bartlett (excerpted pages)

European Patent Application No. EP 2266400 to Gasse et al.

Evidence of publication from file history of U.S. Patent No. 9,732,008 (dated 8/26/14)

Solvay USA Inc.'s Petition for Post-Grant Review

Petitioner Solvay USA Inc.'s Power of Attorney

Curriculum Vitae of Dr. Gribble

Certified Translation of Chinese Patent No. 101200400 B

U.S. Patent No. 4,530,714 to Kolc et al.

U.S. Patent No. 5,352,265 to Weston et al.

Santa Cruz Biotechnology Ltd of California website located at http://www.scbt.com/datasheet-218975-n-n-butylthiophosphoric-triamide.html

Vemula et al., ¿¿¿Solubility Enhancement Techniques¿¿¿

Chinese Patent No. 101200400 B (Native Language)

U.S. Patent Publication No. 2008/0287709 to Huttenloch et al.

Smale, DMSO ¿¿¿ Agricultural Solvent ¿¿¿ Penetrant-Carrier ¿¿¿ Antiviral Agent, The Sulphur Institute Journal (1969)

Introduction to Organic Chemistry, A. Streitwieser, C. H. Heathcock, E. M. Kosower, 1992, 4th ed., Macmillan (excerpted pages)

Arkema Press Release regarding DMSO website (dated 11/24/2009)

Abraham et al., Proton and Carbon-13 NMR Spectroscropy